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What to Send a Buyer to Prove a Batch of Chromatography Silica

Seven documents. Send them unprompted and the technical objections never arrive.

Seven documents: a batch certificate of analysis, an SDS, a technical data sheet, a particle-size distribution, a BET surface area report, a pH and loss-on-drying record, and — when the buyer is running a method — a test chromatogram. The pack costs nothing extra to assemble and it closes most quality conversations before they start.

The pack

#DocumentWhat the buyer does with it
1Certificate of Analysis (per batch)ties the batch to their order — the single most requested document
2Safety Data SheetEHS clearance and customs handling
3Technical Data Sheetthe standing specification, not batch-specific
4Particle-size distributionconfirms the mesh and micron window (e.g. 40–63 µm)
5BET surface area report, per ISO 9277capacity benchmark; must be consistent with the pore diameter
6pH and loss on drying / water contentreproducibility, and the link to remaining adsorption activity
7Test chromatogramproves the material works in a real separation, not only on paper

The certificate fields that matter

A certificate with only a surface area number is not a characterisation. Insist on all of these:

How to present it so it gets accepted

Quick rejection list

Red flagWhy it fails
Surface area quoted with no methodyou cannot tell what was measured
A 60 Å grade claiming the same surface area as a 100 Å gradepore diameter and surface area move in opposite directions
Particle size given only as "fine powder"no window and no control
Certificate not tied to a batch numbercannot be filed in a quality record
SDS missingblocks customs and EHS clearance

Sources and Standards

Who wrote this page, how, and why.

Written by the VEN Desiccant export team from the ISO 9277 and USP〈621〉references and from the document requests we actually receive from chromatography buyers. Drafting was AI-assisted; the standard references were checked against the published sources and edited by our team before publication. We publish it because most rejected shipments are rejected on paperwork, not on material. Ask us for the batch pack and we will return it filled in for the grade you are specifying.

Last checked: 11 October 2026.

Want the batch pack template?

Send the grade you are specifying and we will return the certificate set filled in for that product.

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